Difference between revisions of "Team:Tuebingen/Demonstrate"

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The Synthesis was not completed. The second step did not work, more correct no reaction took place. We thought that changing the conditions of the reaction could lead to a positive outcome.
 
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Another way to improve the results could be a new approach as whole. Because of the alken as by-product, the yield was alway very small. If one did choose the alken as product, targeting it with an S-Nucleophilic, the yield could be improved.
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The drying of the Azid-Donor is also critical, as the donor decomposes in vacuo and under heat. As it’s a non-explosive and air-stable salt, maybe drying it in a desiccator could be a solution. Nonetheless, the Donor is instabel as long it’s not completely dry and must be handled with care.
 
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Revision as of 15:05, 15 October 2018

Results

Success isn't about the end result, it's about what you learn along the way.- Vera Wang
Placeholder
Chemestry
The Synthesis was not completed. The second step did not work, more correct no reaction took place. We thought that changing the conditions of the reaction could lead to a positive outcome. Another way to improve the results could be a new approach as whole. Because of the alken as by-product, the yield was alway very small. If one did choose the alken as product, targeting it with an S-Nucleophilic, the yield could be improved. The drying of the Azid-Donor is also critical, as the donor decomposes in vacuo and under heat. As it’s a non-explosive and air-stable salt, maybe drying it in a desiccator could be a solution. Nonetheless, the Donor is instabel as long it’s not completely dry and must be handled with care.
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Some Image
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Bioinformatics